Spectral assignments and reference data - Complete assignments of H-1 and C-13 NMR data for 10 phenylethanoid glycosides

Ten phenylethanoid glycosides, including two new ones, isolated from the aerial parts of the mangrove plant Acanthus ilicifolius were identified. The first complete assignments of the H-1 and C-13 NMR chemical shifts for these glycosides were achieved by means of 2D NMR techniques, including H-1-H-1...

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Published inMagnetic resonance in chemistry Vol. 42; no. 7; pp. 659 - 662
Main Authors Wu, J, Huang, JS, Xiao, Q, Zhang, S, Xiao, ZH, Li, QX, Long, LJ, Huang, LM
Format Journal Article
LanguageEnglish
Published HOBOKEN Wiley 01.07.2004
Subjects
Chemistry
Chemistry, Multidisciplinary
Chemistry, Physical
Physical Sciences
Science & Technology
Spectroscopy
Technology
complete NMR assignments
NMR
Acanthus ilicifolius
H-1 NMR
ALCOHOL
2D NMR
GLUCOSIDES
phenylethanoid glycoside
C-13 NMR
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Summary:Ten phenylethanoid glycosides, including two new ones, isolated from the aerial parts of the mangrove plant Acanthus ilicifolius were identified. The first complete assignments of the H-1 and C-13 NMR chemical shifts for these glycosides were achieved by means of 2D NMR techniques, including H-1-H-1 COSY, TOCSY, HSQC and HMBC spectra. Copyright (C) 2004 John Wiley Sons, Ltd.
ISSN:0749-1581
1097-458X
DOI:10.1002/mrc.1393