Synthetic transformation of 1,3-diarylisobenzofuran-DMAD adducts: a facile preparation of tri-substituted α-naphtholsElectronic supplementary information (ESI) available: Copies of 1H and 13C spectra of compounds. CCDC 997379, 1450132, 1438503, 1450133 and 1438209. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6ob00628k

1,3-Diarylisobenzofuran-DMAD adducts upon reaction with BF 3 ·OEt 2 in DCM at room temperature underwent a regiospecific 1,2-aryl migration followed by the Krapcho decarboxylation to give tri-substituted α-naphthols in good yields. 1,3-Diarylisobenzofuran-DMAD adducts upon reaction with BF 3 ·OEt 2...

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Main Authors Karunakaran, Jayachandran, Nandakumar, Meganathan, Senthil Kumar, Natarajan, Mohanakrishnan, Arasambattu K
Format Journal Article
Published 04.05.2016
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Summary:1,3-Diarylisobenzofuran-DMAD adducts upon reaction with BF 3 ·OEt 2 in DCM at room temperature underwent a regiospecific 1,2-aryl migration followed by the Krapcho decarboxylation to give tri-substituted α-naphthols in good yields. 1,3-Diarylisobenzofuran-DMAD adducts upon reaction with BF 3 ·OEt 2 in DCM at room temperature underwent a regiospecific 1,2-aryl migration followed by the Krapcho decarboxylation to give tri-substituted α-naphthols in good yields.
Bibliography:13
1438209
1438503
10.1039/c6ob00628k
Electronic supplementary information (ESI) available: Copies of
,
1
For ESI and crystallographic data in CIF or other electronic format see DOI
C spectra of compounds. CCDC
and
H and
1450132
1450133
997379
ISSN:1477-0520
1477-0539
DOI:10.1039/c6ob00628k