LED lighting as a simple, inexpensive, and sustainable alternative for Wolff rearrangementsElectronic supplementary information (ESI) available: NMR data and copy of spectra of all compounds. See DOI: 10.1039/c4ra15670f

The Wolff rearrangement is one of the best methods for chain homologation. However, it still suffers from many drawbacks with respect to its practical execution in the laboratory. We wish to demonstrate the use of commercial LED lamps as a sustainable alternative for the classic experimental protoco...

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Bibliographic Details
Main Authors Bernardim, Barbara, Hardman-Baldwin, Andrea M, Burtoloso, Antonio C. B
Format Journal Article
LanguageEnglish
Published 27.01.2015
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Summary:The Wolff rearrangement is one of the best methods for chain homologation. However, it still suffers from many drawbacks with respect to its practical execution in the laboratory. We wish to demonstrate the use of commercial LED lamps as a sustainable alternative for the classic experimental protocols typically used for Wolff rearrangements. The Wolff rearrangement suffers from many drawbacks with respect to its practical execution in the laboratory. Herein, commercial LED lamps are employed as a sustainable alternative for the classic protocols typically used for Wolff rearrangements.
Bibliography:10.1039/c4ra15670f
Electronic supplementary information (ESI) available: NMR data and copy of spectra of all compounds. See DOI
ISSN:2046-2069
DOI:10.1039/c4ra15670f