Synthesis and characterization of ZrFe 2 O 4 @SiO 2 @Ade-Pd as a novel, recyclable, green, and versatile catalyst for Buchwald-Hartwig and Suzuki-Miyaura cross-coupling reactions
This work presents the simple synthesis of a green and novel Palladium based magnetic nanocatalyst with effective catalytic properties and reusability. These heterogeneous catalysts were prepared by the anchoring of Pd(0) on the surface of ZrFe O MNPs coated with a di-substituted adenine (Ade) compo...
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Published in | Scientific reports Vol. 13; no. 1; p. 14728 |
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Main Authors | , , , , , , , , |
Format | Journal Article |
Language | English |
Published |
England
07.09.2023
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Online Access | Get full text |
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Summary: | This work presents the simple synthesis of a green and novel Palladium based magnetic nanocatalyst with effective catalytic properties and reusability. These heterogeneous catalysts were prepared by the anchoring of Pd(0) on the surface of ZrFe
O
MNPs coated with a di-substituted adenine (Ade) compound as a green linker. The as-synthesized ZrFe
O
@SiO
@Ade-Pd MNPs were methodically characterized over different physicochemical measures like VSM, EDX, Map, SEM, TEM, ICP, and FT-IR analysis. The catalytic activity of ZrFe
O
@SiO
@Ade-Pd was carefully examined for the room-temperature Carbon-Carbon coupling reaction in acetonitrile as a solvent. It is worth noting that the synthesized solid catalyst can be easily recovered with a bar magnet and reused for five cycles without decrease of catalytic activity. |
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ISSN: | 2045-2322 |