Synthesis of 10-substituted 3,6-diphenyl-9-aryl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dion e derivatives

A series of novel 10-substituted 3,6-diphenyl-9-aryl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dion e derivatives synthesised by condensation of different amines with xanthenes, was prepared from 5-phenylcyclohexane-1,3-dione and aromatic aldehydes by a Knoevenagel and Michael reaction and cyclisati...

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Published inJournal of chemical research Vol. 39; no. 7
Main Authors Wang, Fang-Ming, Bao, Dan, Hu, Bing-Xiang, Zhou, Ze-Yu, Huang, Deng-Deng, Chen, Li-Zhuang, Dan, Yuan-Yuan
Format Journal Article
LanguageEnglish
Published 01.07.2015
Subjects
Amines
Condensing
Derivatives
Diffraction
Michael reaction
Molecular structure
Synthesis
X-rays
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Summary:A series of novel 10-substituted 3,6-diphenyl-9-aryl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dion e derivatives synthesised by condensation of different amines with xanthenes, was prepared from 5-phenylcyclohexane-1,3-dione and aromatic aldehydes by a Knoevenagel and Michael reaction and cyclisation catalysed by a trace of L-proline at room temperature. In addition, the molecular structure of a xanthene was determined by single-crystal X-ray diffraction analysis.
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ISSN:1747-5198
2047-6507
DOI:10.3184/174751915X14355819348991