Experimental study of FeaCaO based system above 1,000 degree C

• Published in: Journal of thermal analysis and calorimetry Vol. 112; no. 1; pp. 465 - 471
• Main Authors: Zaludova, Monika, Smetana, Bedrich, Zla, Simona, Dobrovska, Jana, Watson, Andy, Vontorova, Jirina, Rosypalova, Silvie, Kukutschova, Jana, Cagala, Michal
• Format: Journal Article
• Language: English
• Published: 01.04.2013
• Subjects: Accessibility; Alloys; Carbon; Differential scanning calorimetry; Differential thermal analysis; Modular; Oxygen content; Phase transformations
• ISSN: 1388-6150; 1572-8943
• DOI: 10.1007/s10973-012-2847-8

The paper deals with the study of phase transformation temperatures of the model FeaCaO based metallic alloys in the high temperature region (above 1,000 degree C). Six model alloys with graded carbon and oxygen content were prepared and studied. Temperatures of phase transitions were obtained using DTA method (differential thermal analysis). The Setaram SETSYS 18ac (TG/DTA/DSC/TMA) modular experimental system was used for measurements. Influence of composition change (carbon and oxygen content) on shift of phase transformation temperatures is investigated in this paper. New original data (phase transformation temperatures) were obtained in this study. Controlled heating of the alloys was conducted at the rates of 2, 4, 7, 10, 15 and 20 degree C min?1. Comparison of the obtained experimental data with the data presented in the literature was also carried out. It follows from comparison of the obtained results with the data accessible in the literature that a lack of experimental data exists, and these available data significantly differ.