Indium Modified Mesoporous Zeolite AlMCM-41 as a Heterogeneous Catalyst for the Knoevenagel Condensation Reaction

The Indium modified mesoporous zeolite AlMCM-41 were synthesized by hydrothermal method and characterized by powder X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS) techniques. The Knoevenagel cond...

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Bibliographic Details
Published inBulletin of the Korean Chemical Society Vol. 31; no. 5; pp. 1301 - 1304
Main Authors Katkar, Santosh S, Lande, Machhindra K, Arbad, Balasaheb R, Rathod, Sandip B
Format Journal Article
LanguageKorean
Published 2010
Subjects
Mesoporous zeolite In/AlMCM-41
Knoevenagel condensation
Heterogeneous catalyst
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Summary:The Indium modified mesoporous zeolite AlMCM-41 were synthesized by hydrothermal method and characterized by powder X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS) techniques. The Knoevenagel condensation of aldehyde with malononitrile or ethyl cyanoacetate was carried out at reflux condition in ethanol by using heterogeneous In/AlMCM-41 catalyst. This method is fast, efficient, easy work-up and eco-friendly to afford the corresponding Knoevenagel adducts. The catalyst was recovered and reused for several cycles with consistent activity.
Bibliography:KISTI1.1003/JNL.JAKO201014752579262
ISSN:0253-2964
1229-5949