Application of Microwave Activation Techniques to the N-Alkenyl Protection of Lactams

Rapid and facile syntheses of N-alkenyl lactam series via condensation between lactams and a variety of aldehydes such as n-propanal, isobutanal, n-butanal, n-hexanal, n-octanal and phenylacetaldehyde were studied under microwave or conventional heating. Various solid catalysts and solvents were exa...

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Published inBulletin of the Korean Chemical Society Vol. 27; no. 2; pp. 286 - 290
Main Authors Kim, Ki-Won, Ahn, Hee-Sook, Lee, Ho-Joon, Song, Suk-Jin, Kim, Chung-Gi, Kwon, Tae-Woo
Format Journal Article
LanguageKorean
Published 2006
Subjects
Ethyl pyroglutamate
Aldehyde condensation
N-Alkenylation
Microwave irradiation
idin-2-one
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Summary:Rapid and facile syntheses of N-alkenyl lactam series via condensation between lactams and a variety of aldehydes such as n-propanal, isobutanal, n-butanal, n-hexanal, n-octanal and phenylacetaldehyde were studied under microwave or conventional heating. Various solid catalysts and solvents were examined to maximize the yields of condensation reactions.
Bibliography:KISTI1.1003/JNL.JAKO200602727013317
ISSN:0253-2964
1229-5949