Soft magnetic phase nanoparticles preparations and associated methods thereof

A method of synthesizing magnetic nanoparticles comprising soft magnetic phases is provided, wherein the method comprises degassing a first mixture at a temperature in a range from about 80° C. to 130° C. The first mixture comprises a solvent, a compound comprising iron, cobalt, or combinations ther...

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Bibliographic Details
Main Authors BONITATIBUS, JR. PETER JOHN, COLBORN ROBERT EDGAR, JOHNSON FRANCIS, KANDAPALLIL BINIL ITTY IPE
Format Patent
LanguageEnglish
Published 02.02.2016
Subjects
BASIC ELECTRIC ELEMENTS
CASTING
ELECTRICITY
INDUCTANCES
MAGNETS
MAKING METALLIC POWDER
MANUFACTURE OF ARTICLES FROM METALLIC POWDER
PERFORMING OPERATIONS
POWDER METALLURGY
SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
TRANSFORMERS
TRANSPORTING
WORKING METALLIC POWDER
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Summary:A method of synthesizing magnetic nanoparticles comprising soft magnetic phases is provided, wherein the method comprises degassing a first mixture at a temperature in a range from about 80° C. to 130° C. The first mixture comprises a solvent, a compound comprising iron, cobalt, or combinations thereof dissolved in the solvent, and an organic component comprising a fatty acid or an amine. Degassing the first mixture is followed by adding a capping ligand to the first mixture under inert atmosphere to form a second mixture; adding a reducing agent to the second mixture at a temperature in a processing temperature range from about 250° C. to about 350° C. to form a third mixture; and incubating the third mixture at a temperature within the processing temperature range to form nanoparticles comprising a soft magnetic phase.
Bibliography:Application Number: US201313788218