MANUFACTURE OF ELONGATED FUSED QUARTZ MEMBER

• Main Authors: GETZENDINER A,US, ANTCZAK S,US, RIGGERT M,US
• Format: Patent
• Language: English
• Published: 09.10.1973
• Subjects: CHEMISTRY; GLASS; MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES; METALLURGY; MINERAL OR SLAG WOOL

1392359 Fused quartz GENERAL ELECTRIC CO 19 April 1972 [22 April 1971] 18212/72 Heading C1M A continuous method of forming an elongated fused quartz member comprising: (A) continuously feeding silicon dioxide in particulate form at a predetermined rate into the top of a heated crucible, (B) fusing said silicon dioxide continuously in an upper heated zone of the crucible supplied with a gas atmosphere of hydrogen and helium containing 40-65% by volume hydrogen, while maintaining a fusion temperature not below 2050‹ C., (C) continuing to heat the fused material in a lower zone of said crucible at a temperature below 2050‹ C., and (D) drawing the fused material continuously from said lower zone of the crucible through forming means in the presence of an atmosphere containing hydrogen in a non-oxidizing carrier gas. In a preferred embodiment (Fig. 1), glass tubing is formed. Silica is fed to the crucible 10 made of tungsten or molybdenum by an automatic feeder means which maintains a predetermined level of material in the crucible via a discharge tube 22 having its outlet opening located in said crucible. The silica being fed into the heated crucible is surrounded by a purge gas consisting of hydrogen and helium supplied by tube 24. The silica melts in the upper zone 14 into which a supply pipe 58 located in the top section of the exterior housing supplies a similar purge gas mixture to the melting zone of the crucible as inlet pipe 24. The lower portion 28 of said crucible includes an annular ring 30 having a central opening 32 through which the fused quartz member is formed by drawing the viscous material. A core 34 is centrally disposed in the opening 32, the hollow interior of which is connected to inlet pipe 38 which enters the crucible at the top thereof and traverses the entire length of said crucible. Inlet pipe 38 supplies a gaseous mixture of hydrogen and a carrier gas such as nitrogen to the interior of the tube as it is being drawn. A second inlet pipe 42 supplies the same gaseous mixture as supplied by pipe 38 to an annular space 44 around the crucible. This space includes a central opening in the bottom through which the elongated fused quartz member, surrounded by the gas supplied by 42, is drawn from the furnace. The exterior wall of said annular space comprises a refractory cylinder 48 and spaced therefrom is the exterior housing 50 of the furnace construction. Between he exterior wall of refractory cylinder 48 and the interior wall of housing 50 are disposed two helical-shaped induction heating coils 54 and 56 for heating the upper and lower zones of the crucible respectively.