Preparation of decahalodiphenyl oxide

This invention provides a process of preparing reaction-derived decahalodiphenyl oxide of high purity. The process comprises cofeeding separate feeds of (a) diphenyl oxide and/or partially brominated diphenyl oxide and (b) bromine chloride, bromine chloride and bromine, or bromine chloride and chlor...

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Bibliographic Details
Main Authors HARKINS, JR, BOONE, JAMES E
Format Patent
LanguageChinese
English
Published 16.03.2008
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Summary:This invention provides a process of preparing reaction-derived decahalodiphenyl oxide of high purity. The process comprises cofeeding separate feeds of (a) diphenyl oxide and/or partially brominated diphenyl oxide and (b) bromine chloride, bromine chloride and bromine, or bromine chloride and chlorine to a refluxing reaction mixture comprising bromine and at least one Lewis acid bromination catalyst so that high purity decahalodiphenyl oxide is formed.
Bibliography:Application Number: TW20070131192