METHOD FOR PREPARING ADJOENE (Z)- AND (E)-ISOMERS IN RATIO 2:1

FIELD: chemical technology. ^ SUBSTANCE: invention relates to a method for preparing mixture of (Z)- and (E)-isomers of adjoin in the ratio 2:1. Solution of synthetic illicit in n-butanol is kept for 6 days at temperature 21-23oC followed by, if necessary, separation of isomers by method of preparat...

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Main Authors KOROLEV V.L, CHERNYSHOVA I.V, ZALEPUGIN D.JU, POLJAKOV V.S, TIL'KUNOVA N.A, L'VOV I.A, MISHIN V.S, KOZLOVA A.E, TOLOKONNIKOVA JU.V
Format Patent
LanguageEnglish
Russian
Published 10.11.2004
Edition7
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Summary:FIELD: chemical technology. ^ SUBSTANCE: invention relates to a method for preparing mixture of (Z)- and (E)-isomers of adjoin in the ratio 2:1. Solution of synthetic illicit in n-butanol is kept for 6 days at temperature 21-23oC followed by, if necessary, separation of isomers by method of preparative HPLC. ^ EFFECT: improved preparing method. ^ 1 tbl, 1 dwg, 1 ex
Bibliography:Application Number: RU20030113228