METHOD OF PREPARING AMINE SALTS OF DITHIOPHOSPHORIC ACID ESTERS
FIELD: organoelemental compounds. SUBSTANCE: to prepare dithiophosphoric acid ester salts, elementary phosphorus interacts with elementary sulfur, aliphatic alcohol or mixture of aliphatic alcohols and phenol, or substituted phenol, or aliphatic alcohol-substituted phenol mixture at molar ratio 1:(2...
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Main Authors | , , , |
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Format | Patent |
Language | English |
Published |
10.09.1999
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Edition | 6 |
Subjects | |
Online Access | Get full text |
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Summary: | FIELD: organoelemental compounds. SUBSTANCE: to prepare dithiophosphoric acid ester salts, elementary phosphorus interacts with elementary sulfur, aliphatic alcohol or mixture of aliphatic alcohols and phenol, or substituted phenol, or aliphatic alcohol-substituted phenol mixture at molar ratio 1:(2-2.2): (2-3):(1-1.2), respectively, at 50 to 140 C until conversion of phosphorus and sulfur is completed. Salts are obtained by using following amines: ammonia, primary, secondary, and tertiary aliphatic, aromatic, and heterocyclic amines, and carboxylic acid amides. EFFECT: simplified synthetic procedure. 4 cl, 1 tbl, 31 ex |
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Bibliography: | Application Number: RU19980113724 |