MANUFACTURE OF CEMENT DISPERSANT

PURPOSE:To obtain a cement dispersant consisting mainly of a cndensate, by the condensation, under inert gas-pressurized state between naphthalenesulfonic acid and formaldehyde to reduce reaction time and markedly decrease the amount of the catalyst, i.e. sulfuric acid to effect easier after-treatme...

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Bibliographic Details
Main Authors OOTAKI YASUHIKO, UNO KAZUO, IMAI KIYOTO
Format Patent
LanguageEnglish
Published 08.06.1983
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Summary:PURPOSE:To obtain a cement dispersant consisting mainly of a cndensate, by the condensation, under inert gas-pressurized state between naphthalenesulfonic acid and formaldehyde to reduce reaction time and markedly decrease the amount of the catalyst, i.e. sulfuric acid to effect easier after-treatment. CONSTITUTION:To naphthalenesulfonic acid, ca. 0.01-0.5 (pref. 0.04-0.4)mol, per mol of the above acid, of sulfuric acid as a catalyst is added and then water of ca. 0.15-0.5 time for the weight of the naphthalene sulfonic acid is added followed by incorporating ea. 0.8-1.2 (pref. 0.9-1.1)mol, in terms of formaldehyde, of ca. 37% formalin to carry out a reaction under a pressure >=0.2 (pref. 0.5- 10)kg/cm G of an inert gas (e.g., nitrogen) at[a. 100-140 (pref. 110-130) deg.C for 2-16 (pref. 3-10)hr, thus obtaining a condensate and its salt C the objective cement dispersant). USE:For the application to concrete, mortor, cement paste, etc.
Bibliography:Application Number: JP19810194569