Metal powders

Non-spherical nickel powder substantially free from carbon is produced by decomposing nickel carbonyl vapour in the substantial absence of water vapour in the hot free space of a decomposer having nitrided steel inner surfaces. The steel surfaces are preferably nitrided by heating them to a high tem...

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Bibliographic Details
Main Authors WEST DE WITT HENRY, LLEWELYN DAVID MYERS
Format Patent
LanguageEnglish
Published 22.03.1967
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Summary:Non-spherical nickel powder substantially free from carbon is produced by decomposing nickel carbonyl vapour in the substantial absence of water vapour in the hot free space of a decomposer having nitrided steel inner surfaces. The steel surfaces are preferably nitrided by heating them to a high temperature (e.g. 500 DEG C.) in the presence of ammonia which may be passed alone into the decomposer or passed with the carbonyl in a previous operation with an optional addition of oxygen. In the latter case the ammonia concentration should not exceed 0.2% by volume in the presence of oxygen since this would cause spherical particles to be produced.
Bibliography:Application Number: GB19650034399