METHOD FOR BREAKING DOWN MICHAEL ADDUCTS CONTAINED IN A FLUID F AND FORMED DURING THE PREPARATION OF ACRYLIC ACID

The present invention relates to a method of redissociating Michael adducts of acrylic acid present in a liquid F in a redissociation apparatus comprising at least one separating column K, an evaporator V and a pump P, wherein, in the event of an unwanted rise in the viscosity of the residue R in th...

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Bibliographic Details
Main Authors GIESHOFF, Tile, RAITH, Christian, VAN LOOVEREN, Tim, DUERR, Anna Katharina, REIN, Christian, HAMMON, Ulrich, SCHLIEPHAKE, Volker
Format Patent
LanguageEnglish
French
German
Published 15.03.2023
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Summary:The present invention relates to a method of redissociating Michael adducts of acrylic acid present in a liquid F in a redissociation apparatus comprising at least one separating column K, an evaporator V and a pump P, wherein, in the event of an unwanted rise in the viscosity of the residue R in the bottom space of the separating column K, the feed of the liquid F into the redissociation apparatus is stopped, the residue R in the bottom space of the separating column K is diluted and cooled with a solvent 1, and the bottom space of the separating column K is emptied.
Bibliography:Application Number: EP20210720516