METHOD OF MAKING METAL-LIGAND COMPLEXES

Embodiments of the present disclosure are directed towards method of making a metal-ligand complex, the method including: reacting a (L1)H compound and a base in a primary solvent to make a reaction mixture comprising an intermediate anionic L1 compound in the primary solvent; and reacting the inter...

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Bibliographic Details
Main Authors NAGEL, Pamela D, KUHLMAN, Roger L
Format Patent
LanguageEnglish
French
German
Published 09.03.2022
Subjects
ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
COMPOSITIONS BASED THEREON
MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVINGCARBON-TO-CARBON UNSATURATED BONDS
METALLURGY
ORGANIC CHEMISTRY
ORGANIC MACROMOLECULAR COMPOUNDS
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
THEIR PREPARATION OR CHEMICAL WORKING-UP
THEIR RELEVANT APPARATUS
TRANSPORTING
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Summary:Embodiments of the present disclosure are directed towards method of making a metal-ligand complex, the method including: reacting a (L1)H compound and a base in a primary solvent to make a reaction mixture comprising an intermediate anionic L1 compound in the primary solvent; and reacting the intermediate anionic L1 compound and a L2MX3 complex to make a L1L2MX2 complex, wherein L1 and L2 independently are cyclopentadienyl-type (Cp-type) ligands, M is zirconium or hafnium, and each X is a halide and wherein the intermediate anionic L1 compound is not isolated from the reaction mixture.
Bibliography:Application Number: EP20200728839