METHOD FOR PRODUCING A SPINNABLE SILICA SOL MATERIAL

• Main Authors: BARTH, EKKEHARD, MAHR, BASTIAN
• Format: Patent
• Language: English; French; German
• Published: 28.05.2014
• Subjects: ARTIFICIAL STONE; CEMENTS; CERAMICS; CHEMISTRY; COMPOSITIONS BASED THEREON; COMPOSITIONS OF MACROMOLECULAR COMPOUNDS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDINGMATERIALS; CONCRETE; LIME, MAGNESIA; MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS; METALLURGY; ORGANIC MACROMOLECULAR COMPOUNDS; REFRACTORIES; SLAG; THEIR PREPARATION OR CHEMICAL WORKING-UP; TREATMENT OF NATURAL STONE

In a process for producing a spinnable silica sol material, a viscosity value VS is stipulated which the spinnable silica sol material should have after ripening. A viscosity value VR corresponding to VS which the silica sol material has before ripening is ascertained. An aqueous acid solution and a hydrolysable silicon compound are combined. The combined mixture is evaporated to give a single-phase solution while measuring the viscosity of the mixture and the evaporation process is terminated upon reaching the viscosity value VR. The single-phase solution thus obtained is then ripened to give a silica sol material with the viscosity value VS. The process exhibits reduced waste and more exact reproducibility of the spinning sol properties during the synthesis and an increased space-time yield in the production of biologically degradable and/or resorbable fibers and nonwoven fabrics.