METHOD FOR PRODUCING WATER-ABSORBING RESIN
Object The main object of the present invention is to provide a method for producing water-absorbent resin having reduced discoloration resulting from high-temperature treatment, small amounts of fine powder and coarse powder, and a narrow particle size distribution. Means for achieving the object A...
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Main Authors | , , , |
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Format | Patent |
Language | English French German |
Published |
23.10.2013
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Subjects | |
Online Access | Get full text |
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Summary: | Object The main object of the present invention is to provide a method for producing water-absorbent resin having reduced discoloration resulting from high-temperature treatment, small amounts of fine powder and coarse powder, and a narrow particle size distribution. Means for achieving the object A method for producing water-absorbent resin, comprising:
(1) Step 1, in which a water-soluble ethylenically unsaturated monomer is subjected to a reversed-phase suspension polymerization in a petroleum hydrocarbon dispersion medium in which a surfactant is dissolved, thereby forming a slurry in which primary particles are dispersed, and
(2) Step 2, in which the slurry obtained in Step 1 is cooled to partially precipitate the surfactant, and then a (water-soluble ethylenically unsaturated monomer is polymerized in the slurry to agglomerate the primary particles, thereby forming water-absorbent resin,
wherein the surfactant is a sucrose fatty acid ester in which the monoester content is 25% by mass or less, the tetraester content is 10% by mass or more, and the content of tetra or higher esters is 30% by mass or less. |
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Bibliography: | Application Number: EP20110849751 |