Process for the cleaning of a rectification column

A process for the rectification and sepn. of unsatd. carboxylic acids (I) from the solvents in which (I) are absorbed after the synthesis reaction. The process involves interrupting the rectification and flushing out the rectification column with basic soln.

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Bibliographic Details
Main Authors HAMMON, ULRICH, SCHLIEPHAKE, VOLKER, RAUH, ULRICH, PIES, WOLFGANG
Format Patent
LanguageEnglish
French
German
Published 10.04.2002
Edition7
Subjects
ACYCLIC OR CARBOCYCLIC COMPOUNDS
APPARATUS THEREFOR
CHEMISTRY
GENERAL METHODS OF ORGANIC CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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Summary:A process for the rectification and sepn. of unsatd. carboxylic acids (I) from the solvents in which (I) are absorbed after the synthesis reaction. The process involves interrupting the rectification and flushing out the rectification column with basic soln.
Bibliography:Application Number: EP19960115457