Manufacture of mixed crystals and solid solutions of 1,4-diketopyrrolopyrroles
Prepn. of mixed crystals or solid solns. of 1,4-diketopyrrolo(3,4-c)pyrroles, consisting of 2 different cpds. of formula (I), comprises heating a mixt of these cpds. in solid form to 220-380 degrees C; in which A, B = pyridyl, pyrimidin-4-yl, thienyl, furyl or an opt. substd. phenyl, naphthyl or bri...
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Main Authors | , , , |
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Format | Patent |
Language | English French German |
Published |
01.04.1998
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Edition | 6 |
Subjects | |
Online Access | Get full text |
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Summary: | Prepn. of mixed crystals or solid solns. of 1,4-diketopyrrolo(3,4-c)pyrroles, consisting of 2 different cpds. of formula (I), comprises heating a mixt of these cpds. in solid form to 220-380 degrees C; in which A, B = pyridyl, pyrimidin-4-yl, thienyl, furyl or an opt. substd. phenyl, naphthyl or bridged biphenylyl gp. of the formula (a) - (c). R1, R2 = H, halogen, 1-18 C alkyl, 1-18 C alkoxy, 1-18 C alkylmercapto, 1-18 C alkylamino, 2-18 C alkoxycarbonyl, 2-18 C alkylaminocarbonyl, -CN, -NO2, phenyl, CF3, 5-6 C cycloalkyl, -C=N(1-18 C alkyl), (benz)imidazolyl, pyrazolyl, triazolyl, piperazinyl, (benz)oxazolyl, benzothiazolyl, morpholinyl, piperidyl, pyrrolidinyl or gp. of the formula (d). G = -CH2-, -CHMe-, -CMe2-, -CH=N-, -O-, -S-, -SO-, -SO2-, -CONH- or -NR7-; R3, R4 = H, halogen, 1-6 C alkyl, 1-18 C alkoxy or CN; R5, R6 = H. halogen or 1-6 C alkyl; R7 = H or 1-6 C alkyl. |
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Bibliography: | Application Number: EP19960810602 |