Hermetisch abgedichteter, miniaturisierter Entladungsionisierungsdetektor

• Main Authors: ABDEL-RAHMAN, MAHMOUD F, BAKER, JAMES W, WARCHOL, ANDREW M
• Format: Patent
• Language: German
• Published: 18.05.2006
• Subjects: BASIC ELECTRIC ELEMENTS; ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS; ELECTRICITY; INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES; MEASURING; PHYSICS; TESTING

An apparatus for and method of making a discharge ionization detector. The apparatus comprises a detector body, a detector cavity, located in the detector body and having a discharge electrode and an second discharge electrode, wherein an electric discharge runs between the second discharge electrode and the discharge electrode, and a signal electrode which attracts ionized molecules, an inlet interface, through which a discharge gas enters the detector, an analyte inlet, through which the analyte enters the detector cavity, and an outlet through which the analyte and discharge gas exit the detector body, wherein the apparatus is hermetically sealed. The apparatus is hermetically sealed by vacuum brazing the components to the detector body. The present invention can also have a detector volume as small as 10 micro-liters or less. The method comprises machining a body material to form a detector body, by forming a detector cavity, a column bore and a plurality of electrode bores, preparing the body surface for bonding, and bonding a plurality of electrodes, an inlet interface, a column interface and a vent interface to the detector body, whereby a hermetically sealed system is formed that has a detection zone volume of approximately 5-100 micro-liters.