Process for preparing multicomponent composite rare-earth-tungsten electrode material

The present invention belongs to the field of refractory RE functional material. The improved multicomponent composite RE-W electrode material contains three kinds of RE oxides in 2.0-2.2 wt%, including La2O3, Y2O3 and CeO2 in 0.4-1.4 wt% each, except W. The preparation process of the multicomponent...

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Bibliographic Details
Main Authors BINGSHAN LI, FUCHENG HU, ZUOREN NIE
Format Patent
LanguageEnglish
Published 02.03.2005
Edition7
Subjects
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Summary:The present invention belongs to the field of refractory RE functional material. The improved multicomponent composite RE-W electrode material contains three kinds of RE oxides in 2.0-2.2 wt%, including La2O3, Y2O3 and CeO2 in 0.4-1.4 wt% each, except W. The preparation process of the multicomponent composite RE-W electrode material includes compounding mixed RE oxide solution with La2O3, Y2O3 and CeO2; preparing suspension of ammonium paratungstate in deionized water; mixing the solution and the suspension via stirring, evaporation and drying; the first hydrogen reduction at 550-700 deg.c, and the second hydrogen reduction at 850-1000 deg.c to prepare powder of average granularity of 1.2-1.4 micron. The preparation process has no ammonium paratungstate calcinating step, simplified process, low power consumption, raised finished product rate and stability.
Bibliography:Application Number: CN2004180295