Method for preparing bis (trifluoromethanesulfonyl) imine ionic liquid

The invention relates to a method for preparing a bis (trifluoromethanesulfonyl) imine ionic liquid. The method comprises the following steps: S1, weighing bis (trifluoromethanesulfonyl) imine and a first part of an organic solvent, and uniformly stirring and mixing the bis (trifluoromethanesulfonyl...

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Main Authors YAO BINGJIE, LI HONGLIN, LUO JIANZHI, YANG XIANKUI, SHA TING, SUN AOQI, LI SULING, SHEN YONGMING
Format Patent
LanguageChinese
English
Published 12.07.2024
Subjects
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
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Abstract The invention relates to a method for preparing a bis (trifluoromethanesulfonyl) imine ionic liquid. The method comprises the following steps: S1, weighing bis (trifluoromethanesulfonyl) imine and a first part of an organic solvent, and uniformly stirring and mixing the bis (trifluoromethanesulfonyl) imine and the first part of the organic solvent; s2, weighing a second part of organic solvent, and adding the second part of organic solvent into the reaction kettle; adding organic salt into the reaction kettle; dropwise adding the material obtained in the step S1 into the reaction kettle for reaction; and S3, after the reaction is finished, distilling a mixed solution of the ionic liquid, the bis (trifluoromethanesulfonyl) imine and the organic solvent in the reaction kettle, and recycling the organic solvent and the bis (trifluoromethanesulfonyl) imine to obtain the bis (trifluoromethanesulfonyl) imine ionic liquid in the reaction kettle. The bis (trifluoromethanesulfonyl) imine and the organic salt are used
AbstractList The invention relates to a method for preparing a bis (trifluoromethanesulfonyl) imine ionic liquid. The method comprises the following steps: S1, weighing bis (trifluoromethanesulfonyl) imine and a first part of an organic solvent, and uniformly stirring and mixing the bis (trifluoromethanesulfonyl) imine and the first part of the organic solvent; s2, weighing a second part of organic solvent, and adding the second part of organic solvent into the reaction kettle; adding organic salt into the reaction kettle; dropwise adding the material obtained in the step S1 into the reaction kettle for reaction; and S3, after the reaction is finished, distilling a mixed solution of the ionic liquid, the bis (trifluoromethanesulfonyl) imine and the organic solvent in the reaction kettle, and recycling the organic solvent and the bis (trifluoromethanesulfonyl) imine to obtain the bis (trifluoromethanesulfonyl) imine ionic liquid in the reaction kettle. The bis (trifluoromethanesulfonyl) imine and the organic salt are used
Author YANG XIANKUI
SUN AOQI
SHA TING
LUO JIANZHI
YAO BINGJIE
SHEN YONGMING
LI SULING
LI HONGLIN
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– fullname: SHEN YONGMING
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DocumentTitleAlternate 一种制备双（三氟甲磺酰）亚胺类离子液体的方法
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Snippet The invention relates to a method for preparing a bis (trifluoromethanesulfonyl) imine ionic liquid. The method comprises the following steps: S1, weighing bis...
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CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
Title Method for preparing bis (trifluoromethanesulfonyl) imine ionic liquid
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