Atmosphere glue mixing equipment and process method for precursor impregnation phase

• Main Authors: JIAO XINGJIAN, TIAN YUELONG, LI JUNPING, WU KUN, HAN BOTAO, YANG XIAOGUANG, ZHANG GUOBING
• Format: Patent
• Language: Chinese; English
• Published: 09.06.2023
• Subjects: MIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING; PERFORMING OPERATIONS; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL; SEPARATION; TRANSPORTING

The invention provides precursor dipping phase atmosphere glue mixing equipment and a process method.The equipment comprises a closed storage bin, a spiral feeding device, an inert atmosphere circulating device, a monitoring device and a heating stirring kettle, and full-process inert atmosphere protection of a precursor dipping phase configuration process can be achieved; a plurality of groups of inert gas valves and inert gas discharge pipeline valves are arranged on the closed storage bin, the spiral feeding device and the heating and stirring kettle, and inert atmosphere circulation in the equipment can be realized by combining a vacuum mechanism; an electromagnetic valve, a pressure sensor, an automatic pressure release valve and an online oxygen content monitoring device are designed. The method is suitable for preparation of the precursor impregnation phase, safe, rapid and uniform heating and blending of the solid precursor and the solvent can be realized, and the quality qualification rate of the pre