Nickel-based magnetic compound material as well as synthesis method and application thereof

• Main Authors: WEI MENGYANG, LIU XIANGXIANG, LIN HONGYAN, LIU BINQIU, LIANG SHUANG, YING JUN, ZHAO GANG, LI YAN, LIU GUOCHENG, ZHANG YANPING
• Format: Patent
• Language: Chinese; English
• Published: 04.05.2018
• Subjects: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY; CHEMISTRY; METALLURGY; PERFORMING OPERATIONS; PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL; THEIR RELEVANT APPARATUS; TRANSPORTING; TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE

The invention relates to a nickel-based magnetic compound material as well as a synthesis method and application thereof. The synthesis method comprises the following steps: adding deionized water into NiCl2.6H2O, N,N'-bis(4-methylene pyridine)benzene-1,4-dicarbonamide and trimesic acid, carrying out hydrothermal reaction in a high pressure reactor, and generating an organic ligand Ni complex [Ni3(4-bmbpd)3(BTC)2(H2O)4].4H2O; and grinding and smashing the Ni complex by adopting an agate mortar, dispersing into ethyl alcohol, grinding by adopting a ball grinding mill, carrying out centrifugal separation to obtain a microcrystalline Ni complex material, placing into a tubular furnace under the protection of nitrogen, and calcining, so that the nickel-based magnetic compound material is obtained. The nickel-based magnetic compound material is applied to photocatalytic degradation of an organic dye pollutant material. The nickel-based magnetic compound material provided by the invention has the advantages that ca