Extraction vanadium recovery process

The invention discloses an extraction vanadium recovery process. Spent vanadium catalysts are subjected to water leaching and reductive acid leaching treatment to obtain VOSO4-containing extracted raw liquid, the raw liquid is subjected to the single-stage extraction, tail liquid concentration, sepa...

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Bibliographic Details
Main Authors LI JIE, LIU MINGHAI, JI XUELIANG, HAO XICAI, WANG DI, JIAO CHAN
Format Patent
LanguageChinese
English
Published 13.10.2017
Subjects
CHEMISTRY
FERROUS OR NON-FERROUS ALLOYS
METALLURGY
PRETREATMENT OF RAW MATERIALS
PRODUCTION AND REFINING OF METALS
TREATMENT OF ALLOYS OR NON-FERROUS METALS
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Summary:The invention discloses an extraction vanadium recovery process. Spent vanadium catalysts are subjected to water leaching and reductive acid leaching treatment to obtain VOSO4-containing extracted raw liquid, the raw liquid is subjected to the single-stage extraction, tail liquid concentration, separate reextraction and back extraction vanadium recovery process, vanadium precipitation is carried out with ammonium hydroxide, and roasting is conducted to produce vanadium pentoxide. Saponified P204 is adopted as a main extraction agent, it is ensured that the pH value of the whole system is within the optimal pH value range in the extraction process, the extraction system can maintain a stable pH value, and the single-stage extraction rate of vanadium is greatly improved to above 96.4%; tetravalent vanadium obtained through extraction can be directly subjected to vanadium precipitation without oxidation, a high-purity vanadium product is produced, the technological process is simplified, and atmosphere pollution
Bibliography:Application Number: CN201710483328