One-pot method for synthesizing tiamulin

The invention discloses a one-pot method for synthesizing tiamulin. According to the method, methylbenzenesulfonate pleuromutilin, diethylamine and ethylene sulfide is subject to an one-pot reaction in a ratio of 1: (1.0 to 1.5) :( 1.0 to 2.0) at room temperature of 50 DEG C to obtain the tiamulin....

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Bibliographic Details
Main Authors WANG WEIJIA, SUN BAOLI, WANG LILI, MA SHASHA, LI BAOLIN, LI FANSHI, LI JIANG
Format Patent
LanguageEnglish
Published 25.03.2015
Subjects
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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Summary:The invention discloses a one-pot method for synthesizing tiamulin. According to the method, methylbenzenesulfonate pleuromutilin, diethylamine and ethylene sulfide is subject to an one-pot reaction in a ratio of 1: (1.0 to 1.5) :( 1.0 to 2.0) at room temperature of 50 DEG C to obtain the tiamulin. The method is convenient to operate, low in cost and environment-friendly, and is suitable for industrial production of the tiamulin.
Bibliography:Application Number: CN20141842597