Synthesis of 1-amino-1,3,3,5,5-pentamethylcyclohexane mesylate

Process for manufacturing 1-amino-1,3,3, 5, 5-pentamethylcyclohexane mesylate comprising step (i): (i) reacting 1-amino-1, 3, 3, 5, 5-pentamethylcyclohexane with methane sulfonic acid in a solvent or a mixture of two or more solvents selected among anisole, cumene; pentane, hexane, heptane, isooctan...

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Main Authors PYERIN MICHAEL, HENRICH MARKUS, KOCSAN PAL, TASI GERGELY, SBROGIO FEDERICO, KOLLER HERBERT, NEGURA SIMONA
Format Patent
LanguageChinese
English
Published 02.05.2012
Subjects
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
HUMAN NECESSITIES
HYGIENE
MEDICAL OR VETERINARY SCIENCE
METALLURGY
ORGANIC CHEMISTRY
PREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
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Summary:Process for manufacturing 1-amino-1,3,3, 5, 5-pentamethylcyclohexane mesylate comprising step (i): (i) reacting 1-amino-1, 3, 3, 5, 5-pentamethylcyclohexane with methane sulfonic acid in a solvent or a mixture of two or more solvents selected among anisole, cumene; pentane, hexane, heptane, isooctane; methyl acetate, propyl acetate, isopropyl acetate, n-butyl acetate, isobutyl acetate; methyl ethyl ketone, methyl isopropylketone, methyl isobutyl ketone; dimethyl sulphoxide; tetrahydrofurane, methyltetrahydrofurane, 1,1-diethoxypropane, 1,1-dimethoxymethane, and 2,2-dimethoxypropane.
Bibliography:Application Number: CN201080016256