Method for preparing pigment yellow

The invention provides a method for preparing pigment yellow 83. The method comprises the following steps: 3, 3'-dichlorobenzidine, 3, 3'-dimethylbenzidine, hydrochloric acid and water are stirred, dissolved and added to sodium nitrite for diazotization, so as to obtain a diazonium solutio...

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Bibliographic Details
Main Authors LU DONGJUN, LI XIUJING, CHEN ZHIWEN, CHEN DOUFANG, ZHAN XIUTAO
Format Patent
LanguageChinese
English
Published 11.03.2009
Subjects
ADHESIVES
CHEMISTRY
DYES
LAKES
METALLURGY
MISCELLANEOUS APPLICATIONS OF MATERIALS
MISCELLANEOUS COMPOSITIONS
MORDANTS
NATURAL RESINS
ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES
PAINTS
POLISHES
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Summary:The invention provides a method for preparing pigment yellow 83. The method comprises the following steps: 3, 3'-dichlorobenzidine, 3, 3'-dimethylbenzidine, hydrochloric acid and water are stirred, dissolved and added to sodium nitrite for diazotization, so as to obtain a diazonium solution; a sodium hydroxide solution containing 4-chlorine-2, 5-dimethoxy acetyl acetanilide is dripped into an acetic acid solution at the temperature between 20 and 40 DEG C, so as to prepare a coupling solution; the acetic acid solution contains an emulsion formed by well mixing anionic surfactant, nonionic surfactant, solvent and water; the diazonium solution is dripped into the coupling solution within 1 to 5 hours; the emulsion formed by compounding the anionic surfactant and non-polar hyper-dispersant is added to the coupling solution, reacts for 1 hour, and is heated to 90 to 100 DEG C; polyethylene wax is added in the mixture; and then the mixture, is insulated for 1 to 3 hours, pumped, filtered, washed, dried and ground,
Bibliography:Application Number: CN20071112920