Method for preparing sheet-like microcrystal cellulose and modification processing method

This invention relates to preparation method of a flakiness microcrystalline cellulose, as well as its surface reshaping method. The process: in water disperse medium, take reaction with sulfuric acid to gain flakiness microcrystalline cellulose, then surface by acetic acid esterification or SAA abs...

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Bibliographic Details
Main Authors HU YUCAI, HUANG BAIYONG, GAO SHANMIN, XU YANBIN, DENG JINHUI, WANG YUBAO
Format Patent
LanguageChinese
English
Published 11.05.2011
Subjects
CHEMISTRY
COMPOSITIONS BASED THEREON
DERIVATIVES THEREOF
METALLURGY
ORGANIC MACROMOLECULAR COMPOUNDS
POLYSACCHARIDES
THEIR PREPARATION OR CHEMICAL WORKING-UP
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Summary:This invention relates to preparation method of a flakiness microcrystalline cellulose, as well as its surface reshaping method. The process: in water disperse medium, take reaction with sulfuric acid to gain flakiness microcrystalline cellulose, then surface by acetic acid esterification or SAA absorption modifing, repass wash, filter , dryness, gain the product. The mass ratio of water and cellulose is 3 to 25:1, sulfuric acid volumetric concentration for 30 to 80%, temperature for 10 - to 85 deg, time for 5 to 120 minutes. The mass ratio of acetic ester modifier or SAA and microcrystalline cellulose is 0.1 to 5: 100. The modifier not only keep the favorable physics and mechanical property of cellulose, but also improve dispersibility, greatly advance consistency with high molecular material, broaden the application area.
Bibliography:Application Number: CN2007195908