Method for purifying and refining epsi-caprolactam

This invention relates to a refine means of epsilon - caprolactam by separation and purification. The feature of the invention is that it includes the step of crystallize epsilon - caprolactam from ethereal solution containing crude epsilon - caprolactam. The product purity can reach 99.98%upwards,...

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Bibliographic Details
Main Authors YANG KEYONG, CHEN SHIBIAO, WU WEI, MIN ENZE, WANG ENQUAN, ZHANG SHUZHONG, SUN BIN
Format Patent
LanguageChinese
English
Published 25.01.2012
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Summary:This invention relates to a refine means of epsilon - caprolactam by separation and purification. The feature of the invention is that it includes the step of crystallize epsilon - caprolactam from ethereal solution containing crude epsilon - caprolactam. The product purity can reach 99.98%upwards, absorption value of potassium permanganate is greater than 10000 or more, the extinction value of epsilon - caprolactam at 290nm wavelength is 0.05 or smaller. The invention wholly meets the require of industrial product.
Bibliography:Application Number: CN2006180704