PROCESS FOR THE PREPARATION OF N,N-DIISOPROPYL-2- BENZOTHIAZYL-SULFENAMIDE

PROCESS FOR THE PREPARATION OF N,N-DIISOPROPYL-2-BENZOTHIAZYL-SULFENAMIDE There is disclosed a process for the preparation of N,N-diisopropylbenzothiazyl-2-sulfenamide which comprises contacting an aqueous mixture of diisopropylamine and 2-mercaptobenzothiazole with an oxidizing agent in the presenc...

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Bibliographic Details
Main Author ROLLICK, KEVIN L
Format Patent
LanguageEnglish
French
Published 05.06.1990
Edition4
Subjects
CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
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Summary:PROCESS FOR THE PREPARATION OF N,N-DIISOPROPYL-2-BENZOTHIAZYL-SULFENAMIDE There is disclosed a process for the preparation of N,N-diisopropylbenzothiazyl-2-sulfenamide which comprises contacting an aqueous mixture of diisopropylamine and 2-mercaptobenzothiazole with an oxidizing agent in the presence of sufficient acid to neutralize the excess base, if any, in the oxidizing agent wherein the molar ratio of diisopropylamine to 2-mercaptobenzothiazole is at least 1.5 to 1.
Bibliography:Application Number: CA19860503246