New N-Mannich bases

Amides, aldehydes and benzotriazole or morpholine react, with the elimination of water to form N-Mannich bases or N,N'-arylidene symmetrical diamides in good or very good yields. We also found that amides, aldehydes and 1,2,4-triazole react to form a new N-[1-(1H-1,2,4-triazol-1-yl)alkyl]amides...

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Bibliographic Details
Published inPolish journal of chemistry Vol. 70; no. 9; pp. 1135 - 1142
Main Authors Pernak, J, Weglewski, J, Szymanska, D
Format Journal Article
LanguageEnglish
Published WARSAW POLISH CHEMICAL SOCIETY 01.09.1996
Subjects
Chemistry
Chemistry, Multidisciplinary
Physical Sciences
Science & Technology
synthesis
N-<1-(BENZOTRIAZOL-1-YL)ALKYL>AMIDES
ROUTE
N-(1-morpholinoalkyl)amide
N-[1-(1H-1,2,4-triazol-1-yl)alkyl]amide
CHEMISTRY
symmetrical diamide
N-[1-(benzotriazol-1-yl)alky]-3-pyridinecarboxamide
VERSATILE AMIDOALKYLATION REAGENTS
BENZOTRIAZOLE
AMIDES
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Summary:Amides, aldehydes and benzotriazole or morpholine react, with the elimination of water to form N-Mannich bases or N,N'-arylidene symmetrical diamides in good or very good yields. We also found that amides, aldehydes and 1,2,4-triazole react to form a new N-[1-(1H-1,2,4-triazol-1-yl)alkyl]amides with a 58-85% yield.
ISSN:0137-5083