Determination of seven ingredients of different grades Alismatis Rhizoma by QAMS method
The present study is to establish a quantitative analysis of multi-components by single marker(QAMS) for determining contents of seven compositions in Alismatis Rhizoma, alismoxide, alisol C 23-acetate, alisol A, alismol, alisol B, alisol B 23-acetate and 11-deoxy-alisol B. Six relative correction f...
Saved in:
Published in | Zhongguo zhongyao zazhi Vol. 44; no. 11; p. 2292 |
---|---|
Main Authors | , , , , , , , |
Format | Journal Article |
Language | Chinese |
Published |
China
01.06.2019
|
Subjects | |
Online Access | Get more information |
Cover
Loading…
Abstract | The present study is to establish a quantitative analysis of multi-components by single marker(QAMS) for determining contents of seven compositions in Alismatis Rhizoma, alismoxide, alisol C 23-acetate, alisol A, alismol, alisol B, alisol B 23-acetate and 11-deoxy-alisol B. Six relative correction factors(RCFs) of alismoxide, alisol C 23-acetate, alisol A, alismol, alisol B and 11-deoxy-alisol B were established in the UPLC method with alisol B 23-acetate as the internal standard, which was to calculate the mass fraction of each. The mass fraction of seven effective constituents in Alismatis Rhizoma was calculated by the external standard method(ESM) at the same time. Compared with the content results determined by the ESM and QAMS, the feasibility and accuracy of QAMS method were verified. Within the linear range, the RCFs of alismoxide, alisol C 23-acetate, alisol A, alismol, alisol B, 11-deoxy-alisol B were 0.946, 4.183, 0.915, 1.039, 0.923 and 1.244, respectively, with good repeatability in different expe |
---|---|
AbstractList | The present study is to establish a quantitative analysis of multi-components by single marker(QAMS) for determining contents of seven compositions in Alismatis Rhizoma, alismoxide, alisol C 23-acetate, alisol A, alismol, alisol B, alisol B 23-acetate and 11-deoxy-alisol B. Six relative correction factors(RCFs) of alismoxide, alisol C 23-acetate, alisol A, alismol, alisol B and 11-deoxy-alisol B were established in the UPLC method with alisol B 23-acetate as the internal standard, which was to calculate the mass fraction of each. The mass fraction of seven effective constituents in Alismatis Rhizoma was calculated by the external standard method(ESM) at the same time. Compared with the content results determined by the ESM and QAMS, the feasibility and accuracy of QAMS method were verified. Within the linear range, the RCFs of alismoxide, alisol C 23-acetate, alisol A, alismol, alisol B, 11-deoxy-alisol B were 0.946, 4.183, 0.915, 1.039, 0.923 and 1.244, respectively, with good repeatability in different expe |
Author | Chu, Ke-Dan Lin, Qing-Qing Zhang, Su-Ping Tai, Yan-Ni Wu, Shui-Sheng Xu, Wen Weng, Yan-Hong Li, Xiao-Yan |
Author_xml | – sequence: 1 givenname: Yan-Ni surname: Tai fullname: Tai, Yan-Ni organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China Centre of Biomedical Research & Development, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China – sequence: 2 givenname: Yan-Hong surname: Weng fullname: Weng, Yan-Hong organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China Centre of Biomedical Research & Development, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China – sequence: 3 givenname: Su-Ping surname: Zhang fullname: Zhang, Su-Ping organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China Centre of Biomedical Research & Development, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China – sequence: 4 givenname: Wen surname: Xu fullname: Xu, Wen organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China Centre of Biomedical Research & Development, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China – sequence: 5 givenname: Xiao-Yan surname: Li fullname: Li, Xiao-Yan organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China – sequence: 6 givenname: Qing-Qing surname: Lin fullname: Lin, Qing-Qing organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China – sequence: 7 givenname: Ke-Dan surname: Chu fullname: Chu, Ke-Dan organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China Centre of Biomedical Research & Development, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China – sequence: 8 givenname: Shui-Sheng surname: Wu fullname: Wu, Shui-Sheng organization: School of Pharmacy, Fujian University of Traditional Chinese Medicine Fuzhou 350122, China |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31359656$$D View this record in MEDLINE/PubMed |
BookMark | eNo1j0tLw0AcxPdQsbX2K8jiPXF3s4_kGOoTKqIWPJZ9_NNu7W5CNgr10xtRTzO_gRmYMzSJbQSELinJaSU4udrnNr773O5tCDkjtCIFo6MREzSjhNBMFIRN0SIlb0akpBCCnaJpQQtRSSFn6O0aBuiDj3rwbcRtgxN8QsQ-bntwHuKQfkLnmwb6kfC21w4Srg8-hbGT8MvOf7VBY3PEz_XjKw4w7Fp3jk4afUiw-NM5Wt_erJf32erp7mFZr7JOSJkpJRVzldWOKGKUqTgFqsvKGie05KUVXHEmVEMtV46WxhnDmJLMKQcGOJuji9_Z7sMEcJuu90H3x83_QfYNYCVXsA |
ContentType | Journal Article |
DBID | NPM |
DOI | 10.19540/j.cnki.cjcmm.20190321.205 |
DatabaseName | PubMed |
DatabaseTitle | PubMed |
DatabaseTitleList | PubMed |
Database_xml | – sequence: 1 dbid: NPM name: PubMed url: https://proxy.k.utb.cz/login?url=http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed sourceTypes: Index Database |
DeliveryMethod | no_fulltext_linktorsrc |
ExternalDocumentID | 31359656 |
Genre | English Abstract Journal Article |
GroupedDBID | --- -05 123 2B. 5XA 5XF 92F 92I ACGFS ALMA_UNASSIGNED_HOLDINGS CCEZO CIEJG CW9 EBD EMOBN EOJEC F5P MK0 NPM OBODZ P2P SV3 TCJ TGQ U1G U5O |
ID | FETCH-LOGICAL-p566-77672d9cad070b7b941e1a89cbd5a648c5474257f1c47d18bdbb22762d7debe42 |
ISSN | 1001-5302 |
IngestDate | Wed Oct 16 00:47:34 EDT 2024 |
IsPeerReviewed | true |
IsScholarly | true |
Issue | 11 |
Keywords | Alismatis Rhizoma different grades quantitative analysis of multi-components by single marker sesquiterpenes |
Language | Chinese |
LinkModel | OpenURL |
MergedId | FETCHMERGED-LOGICAL-p566-77672d9cad070b7b941e1a89cbd5a648c5474257f1c47d18bdbb22762d7debe42 |
PMID | 31359656 |
ParticipantIDs | pubmed_primary_31359656 |
PublicationCentury | 2000 |
PublicationDate | 2019-Jun |
PublicationDateYYYYMMDD | 2019-06-01 |
PublicationDate_xml | – month: 06 year: 2019 text: 2019-Jun |
PublicationDecade | 2010 |
PublicationPlace | China |
PublicationPlace_xml | – name: China |
PublicationTitle | Zhongguo zhongyao zazhi |
PublicationTitleAlternate | Zhongguo Zhong Yao Za Zhi |
PublicationYear | 2019 |
SSID | ssib001103552 ssib002262858 ssib051368375 ssj0041955 |
Score | 2.2598433 |
Snippet | The present study is to establish a quantitative analysis of multi-components by single marker(QAMS) for determining contents of seven compositions in... |
SourceID | pubmed |
SourceType | Index Database |
StartPage | 2292 |
Title | Determination of seven ingredients of different grades Alismatis Rhizoma by QAMS method |
URI | https://www.ncbi.nlm.nih.gov/pubmed/31359656 |
Volume | 44 |
hasFullText | |
inHoldings | 1 |
isFullTextHit | |
isPrint | |
link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwnV1Lj9MwELa6IKG9IBDvBeQDt8jLxnGc5LjioQqJClDRFi4rv9IWaFJt28NW--OZiZ00u7AIuETWWI0Sz9fxN848CHmhjRalNoKZI6mYSIRmRW41c4XjRjiuZVNn-_1IDj-Ld5N0Mhhc9LNL1vrQbH-bV_I_WgUZ6BWzZP9Bs91NQQBj0C9cQcNw_Ssdv25jWVrat8J6TBHsRmcOI7l8nEbbA2UdTc-Udavo-Md8hUR1FX3CiLuFQg76EV1630-6T1i_zupqOt3U0RYH5woGajub7xz-Jhrgi6rYqBOeOG9AUDqsw9Z46XB6wz7Md_LJpon0C0lp4QgCs57aUKlgNTEuC9sP9c2qL-vYwifuG0nu29_9Yr0LoI-N-TbV9_mh-WYWWCsAKEvC0ZVP-z8CTSwXjV6TOEkL6cuT_3n2SmXtdmqP7GU5WsdR76QHaBFQsd4XZ47Jpp2tSuNEgm_fuVoCHj5tvqyHpQgFbvGVXl77QvvkVvsQV9yaht6M75DbwS-hxx5kd8lgO7tHTi4BjNYlbQBGewBDYQcw6gFGO4DRADCqzykCjHqA3Sfjt2_Gr4YsdOJgS6D7DCs-cVsYZWGD0JkuROxilRdG21RJkZtUZGj7y9iIzMa5tlpzDtuszSwYCcEfkBtVXblHhMryKM-ARcINhOBZrIo0T6Q1ubNOKuMek4d-GU6XvtrKabtAT66dOSD7O1Q-JTdL-Hu7Z8AV1_p5o9SfZK9iow |
link.rule.ids | 786 |
linkProvider | National Library of Medicine |
openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=Determination+of+seven+ingredients+of+different+grades+Alismatis+Rhizoma+by+QAMS+method&rft.jtitle=Zhongguo+zhongyao+zazhi&rft.au=Tai%2C+Yan-Ni&rft.au=Weng%2C+Yan-Hong&rft.au=Zhang%2C+Su-Ping&rft.au=Xu%2C+Wen&rft.date=2019-06-01&rft.issn=1001-5302&rft.volume=44&rft.issue=11&rft.spage=2292&rft_id=info:doi/10.19540%2Fj.cnki.cjcmm.20190321.205&rft_id=info%3Apmid%2F31359656&rft_id=info%3Apmid%2F31359656&rft.externalDocID=31359656 |
thumbnail_l | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=1001-5302&client=summon |
thumbnail_m | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=1001-5302&client=summon |
thumbnail_s | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=1001-5302&client=summon |