Preparation and Characterization of Zr(SO4)2/TiO2 Catalyst

Solid acid Zr(SO4)2/TiO2 catalyst has highly catalytic activity, and has non-corrosiveness to equipment. It is separated from production expediently. As the above advantages, the influence of Zr(SO4)2 loading amount, calcination temperature, and calcination time on the solid acid Zr(SO4)2/TiO2 catal...

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Published inJournal of applied biomaterials & functional materials Vol. 14; no. 1_suppl; pp. 41 - 45
Main Authors Huang, Xin, Gu, Zhenggui, Sun, Hao
Format Journal Article
LanguageEnglish
Published London, England SAGE Publications 04.07.2016
Sage Publications Ltd
Subjects
Catalysis
Catalysts
Catalytic activity
Roasting
Sulfates - chemical synthesis
Sulfates - chemistry
Temperature
Titanium - chemistry
Titanium dioxide
Zirconium
Zirconium - chemistry
Characterization
Methyl palmitate
Solid acid Zr(SO4)2/TiO2
Synthesis
Catalyst
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Summary:Solid acid Zr(SO4)2/TiO2 catalyst has highly catalytic activity, and has non-corrosiveness to equipment. It is separated from production expediently. As the above advantages, the influence of Zr(SO4)2 loading amount, calcination temperature, and calcination time on the solid acid Zr(SO4)2/TiO2 catalyst preparation process is discussed. The experimental condition is optimized by orthogonal test, the result indicate that Zr(SO4)2 load is 65%, calcination temperature is 430°C, and calcination time is 2.5 h. Solid acid catalyst Zr(SO4)2/TiO2 is analyzed and characterized by FT-IR, XRD and SEM. The results will provide the experimental condition for enlarging experimental study.
Bibliography:ObjectType-Article-1
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ISSN:2280-8000
2280-8000
DOI:10.5301/jabfm.5000310