The first observed complex of 11-crown-3 ether. X-ray crystal structure and NMR study of (benzo-11-crown-3)(2)LiNCS

Buchanan et al present the results of an X-ray crystallographic study of (benzo-11-crown-3)2*LiNCS. The complementarity of the X-ray crystallographic method with solid-state 13C NMR spectroscopy is illustrated and the effects of the Li+ ion complexation on the solution 1H and 13C NMR properties are...

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Bibliographic Details
Published inCanadian journal of chemistry Vol. 80; no. 2; p. 148
Main Authors Buchanan, G W, Azad, M, Yap, G P A
Format Journal Article
LanguageEnglish
Published Ottawa Canadian Science Publishing NRC Research Press 01.02.2002
Subjects
Crystallography
Ether
Lithium
Lithium compounds
Molecules
NMR
Nuclear magnetic resonance
Organometallic compounds
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Summary:Buchanan et al present the results of an X-ray crystallographic study of (benzo-11-crown-3)2*LiNCS. The complementarity of the X-ray crystallographic method with solid-state 13C NMR spectroscopy is illustrated and the effects of the Li+ ion complexation on the solution 1H and 13C NMR properties are discussed.
ISSN:0008-4042
1480-3291
DOI:10.1139/V01-204