전착된 나노 결정질 니켈-철 합금의 미세구조 및 물성에 대한 철의 영향

• Published in: Biuletyn Uniejowski Vol. 38; no. 4; pp. 156 - 162
• Main Authors: 변명환(Myung-Hwan Byun), 조진우(Jin-Woo Cho), 송요승(Yo-Seung Song)
• Format: Journal Article
• Language: Korean
• Published: 한국표면공학회 2005
• Subjects: 기계공학; Grain size; Nickel-iron alloy; Internal stress; Roughness; Electroplating; Hardness; Nanocrystalline; nickel-iron alloy
• ISSN: 1225-8024; 2299-8403; 2288-8403

Nickel-iron nanocrystalline alloys with different compositions and grain sizes were fabricated by electro-plating for MEMS devices. The iron content of the deposits was changed by varying the nickel/iron ion ratio in the electrolyte. X-ray diffraction (XRD) analysis was applied for measuring the strength of the texture and grain size of the deposits. The nickel/iron atom ratio of the deposits was analyzed by EDS. The hardness of the alloys was evaluated by Vickers hardness indenter. The internal stress of the deposits was measured by Thin Film Stress Measurement using Stoney's formula. Surface morphology and roughness were investigated by Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM). The results of this study revealed that at a grain size of approximately $17\~24$nm the hardness, internal stress and roughness depend strongly on the iron content. With increasing the iron content, the hardness and internal stress of the deposits increased. An excellent correlation between the increase in the internal stress and the loss of (200) texture was found.