Experimental Studies of the Effective Sintering Temperature on Electrical and Structural Properties of HgBa2Ca2Cu3O8+δ Compound

: The HgBa2Ca2Cu3O8+δ specimens are manufactured via solid status interaction process at various temperature of sintering at ( 1073, 1123 and 1173 ) K. All the specimens in the immediately studied were submited to common constructional description by X - radiation deviation. The X - radiation deviat...

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Published inIOP conference series. Materials Science and Engineering Vol. 871; no. 1
Main Authors Nsaif, Firas Kadhim, Jasim, Kareem Ali, Wadi, Kassim Mahdi, Alshafaay, B., Khazaal, Ahlam Rashid
Format Journal Article
LanguageEnglish
Published Bristol IOP Publishing 01.06.2020
Subjects
Deviation
HgBa
Mercury barium calcium copper oxide
Radiation
Sintering
Sintering temperature
Transition temperature
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Summary:: The HgBa2Ca2Cu3O8+δ specimens are manufactured via solid status interaction process at various temperature of sintering at ( 1073, 1123 and 1173 ) K. All the specimens in the immediately studied were submited to common constructional description by X - radiation deviation. The X - radiation deviation data combined from different samples agree with ( Hg - 1223 ) stages, then the investigations indicated that tetragonal construct for all specimens with an increasing in the dimension c to 15.87 A and reducing the mass density (ρM ) to 1.481 g / cm3 at 1173 K. The four - sensor procedure was achieved to detection the transition temperature ( Ts ), then it raised from 116 K to 121 K with increasing sintering temperature from 1073 K to 1123 K and decreased to 109 K at 1173 K.
ISSN:1757-8981
1757-899X
DOI:10.1088/1757-899X/871/1/012078