Tin-Mediated Route to Polytungstates of RhII and PdII
Three polyoxotungstates of SnII, PdII, and RhII, Na8[H2SnW12O42]·nH2O [1, n = 22.75 (1a) and n = 31.10 (1b)], Na2K(H)[Pd(H2O)4][H2W12O48{Pd(H2O)3}2]·10H2O (2), and Na8[Rh2(H2O)2(W5O18)2]·21.25H2O (3) were obtained. The complexes were characterized by X‐ray analysis, solid‐state 1H NMR spectroscopy,...
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Published in | European journal of inorganic chemistry Vol. 2013; no. 10-11; pp. 1772 - 1779 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
Weinheim
WILEY-VCH Verlag
01.04.2013
WILEY‐VCH Verlag Wiley Subscription Services, Inc |
Subjects | |
Online Access | Get full text |
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Summary: | Three polyoxotungstates of SnII, PdII, and RhII, Na8[H2SnW12O42]·nH2O [1, n = 22.75 (1a) and n = 31.10 (1b)], Na2K(H)[Pd(H2O)4][H2W12O48{Pd(H2O)3}2]·10H2O (2), and Na8[Rh2(H2O)2(W5O18)2]·21.25H2O (3) were obtained. The complexes were characterized by X‐ray analysis, solid‐state 1H NMR spectroscopy, IR spectroscopy, thermogravimetric analysis, and elemental analysis.
Polyoxotungstates of SnII, PdII, and RhII, Na8[H2SnW12O42]·nH2O, Na2K(H)[Pd(H2O)4][H2W12O48{Pd(H2O)3}2]·10H2O, and Na8[Rh2(H2O)2(W5O18)2]·nH2O, were obtained and characterized by X‐ray analysis and solid‐state 1H NMR spectroscopy. |
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Bibliography: | ArticleID:EJIC201201162 ark:/67375/WNG-VL76TSVC-6 istex:80C4A16B02B1C2EBB2082D4A66568F79215907F5 |
ISSN: | 1434-1948 1099-0682 |
DOI: | 10.1002/ejic.201201162 |