A low temperature approach for photo/cathodoluminescent Gd2O2S:Tb (GOS:Tb) nanophosphors
Titrating the aqueous solution of equimolar RE(NO3)3 and (NH4)2SO4 with NH4OH to pH~9 at ~4°C produced an amorphous precursor that yielded phase‐pure and well‐dispersed RE2O2S nanopowder (RE = Gd0.99Tb0.01; GOS:Tb) via a RE2O2SO4 intermediate upon annealing in H2. The powders calcined at the typical...
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| Published in | Journal of the American Ceramic Society Vol. 102; no. 6; pp. 3296 - 3306 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English Japanese |
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| Abstract | Titrating the aqueous solution of equimolar RE(NO3)3 and (NH4)2SO4 with NH4OH to pH~9 at ~4°C produced an amorphous precursor that yielded phase‐pure and well‐dispersed RE2O2S nanopowder (RE = Gd0.99Tb0.01; GOS:Tb) via a RE2O2SO4 intermediate upon annealing in H2. The powders calcined at the typical temperatures of 700/1200°C exhibited unimodal size distributions and have the average crystallize sizes of ~17/55 nm, average particle sizes of ~284/420 nm, and specific surface areas of ~14.62/4.53 m2/g (equivalent particle sizes: ~56/180 nm). The 1200°C product exhibited sharp green luminescence at ~544 nm (FWHM = 2.3 nm; λex = 275 nm), with an absolute quantum yield of ~24.8% and a fluorescence lifetime of ~1.34 ms at room temperature. It was also shown that the powder possesses favorable thermal stability (the activation energy for thermal quenching of luminescence ~0.305 eV) and is stable under electron beam irradiation up to 7 kV and 50 μA. The synthetic technique has the advantages of scalability and favorable dispersion and high chemical/phase purity for GOS powder, which may allow the sintering of scintillation ceramics at lower temperatures.
Gd2O2S:Tb nanophosphor with favorable dispersion and high chemical/phase purity was obtained via a low temperature precipitation approach. |
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| AbstractList | Titrating the aqueous solution of equimolar RE(NO3)3 and (NH4)2SO4 with NH4OH to pH~9 at ~4°C produced an amorphous precursor that yielded phase‐pure and well‐dispersed RE2O2S nanopowder (RE = Gd0.99Tb0.01; GOS:Tb) via a RE2O2SO4 intermediate upon annealing in H2. The powders calcined at the typical temperatures of 700/1200°C exhibited unimodal size distributions and have the average crystallize sizes of ~17/55 nm, average particle sizes of ~284/420 nm, and specific surface areas of ~14.62/4.53 m2/g (equivalent particle sizes: ~56/180 nm). The 1200°C product exhibited sharp green luminescence at ~544 nm (FWHM = 2.3 nm; λex = 275 nm), with an absolute quantum yield of ~24.8% and a fluorescence lifetime of ~1.34 ms at room temperature. It was also shown that the powder possesses favorable thermal stability (the activation energy for thermal quenching of luminescence ~0.305 eV) and is stable under electron beam irradiation up to 7 kV and 50 μA. The synthetic technique has the advantages of scalability and favorable dispersion and high chemical/phase purity for GOS powder, which may allow the sintering of scintillation ceramics at lower temperatures. Titrating the aqueous solution of equimolar RE(NO3)3 and (NH4)2SO4 with NH4OH to pH~9 at ~4°C produced an amorphous precursor that yielded phase‐pure and well‐dispersed RE2O2S nanopowder (RE = Gd0.99Tb0.01; GOS:Tb) via a RE2O2SO4 intermediate upon annealing in H2. The powders calcined at the typical temperatures of 700/1200°C exhibited unimodal size distributions and have the average crystallize sizes of ~17/55 nm, average particle sizes of ~284/420 nm, and specific surface areas of ~14.62/4.53 m2/g (equivalent particle sizes: ~56/180 nm). The 1200°C product exhibited sharp green luminescence at ~544 nm (FWHM = 2.3 nm; λex = 275 nm), with an absolute quantum yield of ~24.8% and a fluorescence lifetime of ~1.34 ms at room temperature. It was also shown that the powder possesses favorable thermal stability (the activation energy for thermal quenching of luminescence ~0.305 eV) and is stable under electron beam irradiation up to 7 kV and 50 μA. The synthetic technique has the advantages of scalability and favorable dispersion and high chemical/phase purity for GOS powder, which may allow the sintering of scintillation ceramics at lower temperatures. Gd2O2S:Tb nanophosphor with favorable dispersion and high chemical/phase purity was obtained via a low temperature precipitation approach. |
| Author | Xiao-Jun Wang Meiting Li Zhihao Wang Qinghong Meng Ji-Guang Li Xuejiao Wang Qi Zhu |
| Author_xml | – sequence: 1 givenname: Xuejiao orcidid: 0000-0003-4327-2340 surname: Wang fullname: Wang, Xuejiao email: wangxuejiao@bhu.edu.cn organization: National Institute for Materials Science – sequence: 2 givenname: Qinghong surname: Meng fullname: Meng, Qinghong organization: Northeastern University – sequence: 3 givenname: Meiting surname: Li fullname: Li, Meiting organization: Northeastern University – sequence: 4 givenname: Xiaojun surname: Wang fullname: Wang, Xiaojun organization: Jiangsu Normal University – sequence: 5 givenname: Zhihao surname: Wang fullname: Wang, Zhihao organization: Northeastern University – sequence: 6 givenname: Qi orcidid: 0000-0001-5513-6309 surname: Zhu fullname: Zhu, Qi organization: Northeastern University – sequence: 7 givenname: Ji‐Guang orcidid: 0000-0002-5625-7361 surname: Li fullname: Li, Ji‐Guang email: li.jiguang@nims.go.jp organization: National Institute for Materials Science |
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| Snippet | Titrating the aqueous solution of equimolar RE(NO3)3 and (NH4)2SO4 with NH4OH to pH~9 at ~4°C produced an amorphous precursor that yielded phase‐pure and... |
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| SubjectTerms | Ammonium hydroxide Ammonium sulfate Aqueous solutions Ceramic powders Electron beams Electron irradiation Fluorescence GOS Low temperature low‐temperature processing Luminescence Nanophosphors nanopowder Organic chemistry oxysulfide Sintering (powder metallurgy) Thermal stability |
| Title | A low temperature approach for photo/cathodoluminescent Gd2O2S:Tb (GOS:Tb) nanophosphors |
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