Universal procedure for the assessment of the reproducibility and the classification of silica-based reversed-phase packings: I. Assessment of the reproducibility of reversed-phase packings

A method is described that has been used since 1985 to assess the quality and reproducibility of several popular reversed-phase packings. Both the precision of the method and the reproducibility of the packing materials are described. The reproducibility of the newer packings surpasses that of the o...

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Bibliographic Details
Published inJournal of Chromatography A Vol. 849; no. 1; pp. 87 - 100
Main Authors Neue, Uwe D, Serowik, Ed, Iraneta, Pam, Alden, Bonnie A, Walter, Thomas H
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 16.07.1999
Elsevier
Subjects
Analytical chemistry
Chemistry
Chromatographic methods and physical methods associated with chromatography
Exact sciences and technology
Other chromatographic methods
Silica
Stationary phases, LC
Silica
Stationary phases, LC
Performance evaluation
Doxepin
Amitriptyline
Chromatographic retention
Toluene
HPLC chromatography
Experimental study
Reversed phase chromatography
Naphthalene
Reproducibility
Classification
Propranolol
Acenaphthene
Chemometrics
Bonded stationary phase
Physicochemical properties
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Summary:A method is described that has been used since 1985 to assess the quality and reproducibility of several popular reversed-phase packings. Both the precision of the method and the reproducibility of the packing materials are described. The reproducibility of the newer packings surpasses that of the older packings. In addition, improved results are achieved today for the packings that existed in 1985.
ISSN:0021-9673
DOI:10.1016/S0021-9673(99)00435-5