Overcoming challenges in 67 Zn NMR: a new strategy of signal enhancement for MOF characterization

Zn solid-state NMR suffers from low sensitivity, limiting its ability to probe the Zn surroundings in MOFs. We report a breakthrough in overcoming challenges in Zn NMR. Combining new cryogenic MAS probe technology and performing NMR experiments at a high magnetic field results in remarkable signal e...

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Published inChemical communications (Cambridge, England) Vol. 59; no. 35; pp. 5205 - 5208
Main Authors Zhang, Wanli, Hassan, Alia, Struppe, Jochem, Monette, Martine, Hung, Ivan, Gan, Zhehong, Martins, Vinicius, Terskikh, Victor, Huang, Yining
Format Journal Article
LanguageEnglish
Published England 27.04.2023
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Summary:Zn solid-state NMR suffers from low sensitivity, limiting its ability to probe the Zn surroundings in MOFs. We report a breakthrough in overcoming challenges in Zn NMR. Combining new cryogenic MAS probe technology and performing NMR experiments at a high magnetic field results in remarkable signal enhancement, yielding enhanced information for MOF characterization.
ISSN:1359-7345
1364-548X
DOI:10.1039/D3CC00716B