High-resolution transmission electron microscopic investigations of molybdenum thin films on faceted α-Al 2 O 3

Epitaxially grown Mo films on a faceted corundum (α-Al 2 O 3 ) m plane were investigated by transmission electron microscopy. Low- and high-resolution images were taken from a cross-section specimen cut perpendicular to the facets. It was possible to identify unambiguously the crystallographic orien...

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Bibliographic Details
Published inJournal of applied crystallography Vol. 38; no. 2; pp. 260 - 265
Main Authors Wiehl, Leonore, Oster, Jens, Huth, Michael
Format Journal Article
LanguageEnglish
Published 01.04.2005
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Summary:Epitaxially grown Mo films on a faceted corundum (α-Al 2 O 3 ) m plane were investigated by transmission electron microscopy. Low- and high-resolution images were taken from a cross-section specimen cut perpendicular to the facets. It was possible to identify unambiguously the crystallographic orientation of these facets and explain the considerable deviation (∼10°) of the experimental interfacet angle, as measured with atomic force microscopy (AFM), from the expected value. For the first time, proof is given for a smooth \{10\bar{1}1\} facet and a curvy facet with orientation near to \{10\bar{1}\bar{2}\}. Moreover, the three-dimensional epitaxial relationship of an Mo film on a faceted corundum m surface was determined.
ISSN:0021-8898
DOI:10.1107/S0021889804033126