Crystal structure of diaqua-bis(μ 2 -6-phenylpyridine-2-carboxylate-κ 3 N,O:O)-bis(6-phenylpyridine-2-carboxylato-κ 2 N,O)lead(II) – N,N -dimethylformamide – water (1/2/4), C 54 H 58 N 6 O 16 Pb 2
Abstract C 54 H 58 N 6 O 16 Pb 2 , triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 9.4690(6) Å, b = 12.9374(6) Å, c = 13.2303(7) Å, V = 1341.90(15) Å 3 , α = 63.395(5)°, β = 74.291(5)°, γ = 69.113(5)°, Z = 1, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0484, T = 150 K.
Saved in:
| Published in | Zeitschrift für Kristallographie. New crystal structures Vol. 236; no. 6; pp. 1199 - 1201 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
20.12.2021
|
| Online Access | Get full text |
Cover
Loading…
| Summary: | Abstract
C
54
H
58
N
6
O
16
Pb
2
, triclinic,
P
1
‾
$P‾{1}$
(no. 2),
a
= 9.4690(6) Å,
b
= 12.9374(6) Å,
c
= 13.2303(7) Å,
V
= 1341.90(15) Å
3
,
α
= 63.395(5)°,
β
= 74.291(5)°,
γ
= 69.113(5)°,
Z
= 1,
R
gt
(
F
) = 0.0284,
wR
ref
(
F
2
) = 0.0484,
T
= 150 K. |
|---|---|
| ISSN: | 1433-7266 2197-4578 |
| DOI: | 10.1515/ncrs-2021-0277 |