ChemInform Abstract: Synthesis and Characterization of Two‐Dimensional Nb 4 C 3 (MXene)

Abstract Phase‐pure, two‐dimensional Nb 4 C 3 T x (T x : general surface termination) is synthesized by immersion of Nb 4 AlC 3 powder (obtained by in situ hot pressing of mixtures of the elements at 3 MPa and 1700 °C for 1 h) in 48‐51% aqueous HF for 96 h at ambient temperature with stirring (77% y...

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Published inChemInform Vol. 45; no. 40
Main Authors Ghidiu, M., Naguib, M., Shi, C., Mashtalir, O., Pan, L. M., Zhang, B., Yang, J., Gogotsi, Y., Billinge, S. J. L., Barsoum, M. W.
Format Journal Article
LanguageEnglish
Published 30.09.2014
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Summary:Abstract Phase‐pure, two‐dimensional Nb 4 C 3 T x (T x : general surface termination) is synthesized by immersion of Nb 4 AlC 3 powder (obtained by in situ hot pressing of mixtures of the elements at 3 MPa and 1700 °C for 1 h) in 48‐51% aqueous HF for 96 h at ambient temperature with stirring (77% yield).
ISSN:0931-7597
1522-2667
DOI:10.1002/chin.201440016