Sonochemical synthesis of 5-substituted 1 H -tetrazoles catalyzed by ZrP 2 O 7 nanoparticles and regioselective conversion into new 2,5-disubstituted tetrazoles

Abstract The ultrasound-assisted preparation of 2-(1 H -tetrazol-5-yl) acrylonitrile derivatives via a one-pot multi-component method is described successfully using ZrP 2 O 7 nanoparticles as a catalyst. Readily available tetrazoles can be transformed into the corresponding 1,5- and 2,5-disubstitut...

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Published inZeitschrift für Naturforschung. B, A journal of chemical sciences Vol. 70; no. 11; pp. 819 - 828
Main Authors Safaei-Ghomi, Javad, Paymard-Samani, Soleiman, Zahedi, Safura, Shahbazi-Alavi, Hossein
Format Journal Article
LanguageEnglish
Published 01.11.2015
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Abstract Abstract The ultrasound-assisted preparation of 2-(1 H -tetrazol-5-yl) acrylonitrile derivatives via a one-pot multi-component method is described successfully using ZrP 2 O 7 nanoparticles as a catalyst. Readily available tetrazoles can be transformed into the corresponding 1,5- and 2,5-disubstituted tetrazoles. 2,4′-Dibromoacetophenone gave the corresponding 2,5-disubstituted derivative as the only isomer. Synthesis of tetrazole derivatives with excellent yields in short times, a wide range of products under ultrasound irradiation, environmental benignity and a simple work-up procedure are some of the important features of this protocol.
AbstractList Abstract The ultrasound-assisted preparation of 2-(1 H -tetrazol-5-yl) acrylonitrile derivatives via a one-pot multi-component method is described successfully using ZrP 2 O 7 nanoparticles as a catalyst. Readily available tetrazoles can be transformed into the corresponding 1,5- and 2,5-disubstituted tetrazoles. 2,4′-Dibromoacetophenone gave the corresponding 2,5-disubstituted derivative as the only isomer. Synthesis of tetrazole derivatives with excellent yields in short times, a wide range of products under ultrasound irradiation, environmental benignity and a simple work-up procedure are some of the important features of this protocol.
Author Zahedi, Safura
Paymard-Samani, Soleiman
Shahbazi-Alavi, Hossein
Safaei-Ghomi, Javad
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  givenname: Hossein
  surname: Shahbazi-Alavi
  fullname: Shahbazi-Alavi, Hossein
  organization: Faculty of Chemistry, Department of Organic Chemistry, University of Kashan, Kashan, PO Box 87317-51167, Iran
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Snippet Abstract The ultrasound-assisted preparation of 2-(1 H -tetrazol-5-yl) acrylonitrile derivatives via a one-pot multi-component method is described successfully...
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Title Sonochemical synthesis of 5-substituted 1 H -tetrazoles catalyzed by ZrP 2 O 7 nanoparticles and regioselective conversion into new 2,5-disubstituted tetrazoles
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