Recent Development of the XANES Spectral Analysis Methods for the Structure Characterization of Metal Complexes in Solution

Recent progress of the XANES (X-ray absorption near-edge structure) spectral analysis methods for the structure characterization of metal complexes (MC) in solution is reviewed. Typical examples showing the scheme of the apparatus for XAFS (X-ray absorption fine structure) data collection, preparati...

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Published inAnalytical Sciences Vol. 24; no. 11; pp. 1385 - 1392
Main Authors KURISAKI, Tsutomu, MATSUO, Shuji, TÓTH, Imre, WAKITA, Hisanobu
Format Journal Article
LanguageEnglish
Published Singapore The Japan Society for Analytical Chemistry 2008
Springer Nature Singapore
Japan Science and Technology Agency
Subjects
Analytical Chemistry
Chemistry
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Summary:Recent progress of the XANES (X-ray absorption near-edge structure) spectral analysis methods for the structure characterization of metal complexes (MC) in solution is reviewed. Typical examples showing the scheme of the apparatus for XAFS (X-ray absorption fine structure) data collection, preparation and handling of solution samples, data treatment and analysis for XANES spectra, and future of XANES spectroscopy are presented. Detailed examples for the apparatus developed for laboratory scale spectrometers for XANES together with a combined spectral analyses using multi scattering method (MS) and molecular orbital (MO) calculation are discussed.
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ISSN:0910-6340
1348-2246
DOI:10.2116/analsci.24.1385