3种桂花浸膏的挥发性物质分析

目的量化分析桂花浸膏的主要挥发性成分,为规范桂花浸膏的质量标准提供基础数据。方法利用固相微萃取（SPME）结合气相色谱-质谱（GC-MS）分析3种浸膏中的挥发性成分,利用谱库、标准品及保留指数对挥发性物质进行定性,并用2-辛醇做内标物,对挥发性物质进行半定量分析。结果共检出51种挥发性物质,主要的挥发性风味物质为酯类、醇类、酮类,其中桂花浸膏1中共检出27种,桂花浸膏2中共检出31种,桂花浸膏3中共检出20种。半定量结果表明桂花浸膏2中挥发性成分含量最高,为959.50 mg/g,桂花浸膏1中挥发性成分含量最低,为89.37 mg/g。结论 3种浸膏中共有的挥发性风味物质分别为反式芳樟醇氧化物...

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Bibliographic Details
Published in食品安全质量检测学报 Vol. 7; no. 4; pp. 1554 - 1560
Main Author 张璟琳 李娟 黄明泉 孙宝国 张玉玉
Format Journal Article
LanguageChinese
Published 北京工商大学理学院化学系,北京,100048%北京食品营养与人类健康高精尖创新中心,北京工商大学,北京 100048 2016
北京工商大学食品质量与安全北京实验室,北京 100048
Subjects
固相微萃取
挥发性物质
桂花浸膏
气相色谱-质谱法
solid phase microextraction
gas chromatography-mass spectrometry
固相微萃取
volatile compounds
桂花浸膏
挥发性物质
气相色谱-质谱法
Osmanthus fragrans extracts
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Summary:目的量化分析桂花浸膏的主要挥发性成分,为规范桂花浸膏的质量标准提供基础数据。方法利用固相微萃取（SPME）结合气相色谱-质谱（GC-MS）分析3种浸膏中的挥发性成分,利用谱库、标准品及保留指数对挥发性物质进行定性,并用2-辛醇做内标物,对挥发性物质进行半定量分析。结果共检出51种挥发性物质,主要的挥发性风味物质为酯类、醇类、酮类,其中桂花浸膏1中共检出27种,桂花浸膏2中共检出31种,桂花浸膏3中共检出20种。半定量结果表明桂花浸膏2中挥发性成分含量最高,为959.50 mg/g,桂花浸膏1中挥发性成分含量最低,为89.37 mg/g。结论 3种浸膏中共有的挥发性风味物质分别为反式芳樟醇氧化物、芳樟醇、2-乙基苯酚、二氢-β-紫罗兰酮、二氢-β-紫罗兰醇、γ-癸内酯、α-紫罗兰酮和β-紫罗兰酮。
Bibliography:ZHANG Jing-Lin;LI Juan;HUANG Ming-Quan;SUN Bao-Guo;ZHANG Yu-Yu; （1. Department of Chemistry, School of Science, Beijing Technology and Business University, Beijing 100048, China; 2. Beo＇ing Higher Institution Engineering Research Center of Food Additives and Ingredients, Beijing Technology and Business University, Beijing 100048, China; 3. Laboratory of Food Quality and Safety, Beijing Technology and Business University, Beijing 100048, China）
11-5956/TS
Objective To detect volatile aroma constituents in Osmanthus fragrans extracts and provide reference data for Osmanthus fragrans extracts quality standards. Methods The volatile components of Osmanthus fragrans extracts were isolated by headspace solid phase microextraction（SPME） and analyzed by gas chromatography-mass spectrometry（GC-MS）. Standard substances and retention index were taken as the qualitative method, while quantification analysis was done by using 2-octanolas（internal standard）. Results A total of 51 kinds of volatile components were identified,
ISSN:2095-0381