P204/正辛醇反胶束萃取L-辛弗林的研究
目的建立一种反胶束萃取L-辛弗林的方法,并验证利用P204/正辛醇萃取L-辛弗林的有效性。方法制备P204/正辛醇反胶束体系萃取枳实L-辛弗林,反萃取液经浓缩干燥后,获得纯化L-辛弗林。利用基于单因素实验进行的正交实验研究最佳分离工艺,通过紫外分析、原子力显微镜表征证实了P204/正辛醇反胶束体系萃取分离L-辛弗林的有效性。结果萃取最佳工艺条件为：水相pH值6.5、萃取时间15 min、P204浓度0.10mol/L、W_0=5,此条件下L-辛弗林的单次萃取率为68.02%,各影响因素影响顺序为：水相pH〉P204浓度〉W_0〉萃取时间。纯化后的L-辛弗林纯度达到87.8%,比原料纯度提升了2...
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| Published in | 食品安全质量检测学报 Vol. 7; no. 4; pp. 1426 - 1431 |
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| Main Author | |
| Format | Journal Article |
| Language | Chinese |
| Published |
菏泽出入境检验检疫局,菏泽,274000%重庆大学化学化工学院,重庆,400044
2016
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| Subjects | |
| Online Access | Get full text |
| ISSN | 2095-0381 |
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| Abstract | 目的建立一种反胶束萃取L-辛弗林的方法,并验证利用P204/正辛醇萃取L-辛弗林的有效性。方法制备P204/正辛醇反胶束体系萃取枳实L-辛弗林,反萃取液经浓缩干燥后,获得纯化L-辛弗林。利用基于单因素实验进行的正交实验研究最佳分离工艺,通过紫外分析、原子力显微镜表征证实了P204/正辛醇反胶束体系萃取分离L-辛弗林的有效性。结果萃取最佳工艺条件为：水相pH值6.5、萃取时间15 min、P204浓度0.10mol/L、W_0=5,此条件下L-辛弗林的单次萃取率为68.02%,各影响因素影响顺序为：水相pH〉P204浓度〉W_0〉萃取时间。纯化后的L-辛弗林纯度达到87.8%,比原料纯度提升了2.9倍。结论该方法为L-辛弗林的分离提取提供一种快速低成本方法,并对其萃取机制及主要变化规律方面提供了基础数据。 |
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| AbstractList | 目的 建立一种反胶束萃取L-辛弗林的方法,并验证利用P204/正辛醇萃取L-辛弗林的有效性.方法 制备P204/正辛醇反胶束体系萃取枳实L-辛弗林,反萃取液经浓缩干燥后,获得纯化L-辛弗林.利用基于单因素实验进行的正交实验研究最佳分离工艺,通过紫外分析、原子力显微镜表征证实了P204/正辛醇反胶束体系萃取分离L-辛弗林的有效性.结果 萃取最佳工艺条件为:水相pH值6.5、萃取时间15 min、P204浓度0.10mol/L、W0=5,此条件下L-辛弗林的单次萃取率为68.02％,各影响因素影响顺序为:水相pH＞P204浓度＞W0＞萃取时间.纯化后的L-辛弗林纯度达到87.8％,比原料纯度提升了2.9倍.结论 该方法为L-辛弗林的分离提取提供一种快速低成本方法,并对其萃取机制及主要变化规律方面提供了基础数据. 目的建立一种反胶束萃取L-辛弗林的方法,并验证利用P204/正辛醇萃取L-辛弗林的有效性。方法制备P204/正辛醇反胶束体系萃取枳实L-辛弗林,反萃取液经浓缩干燥后,获得纯化L-辛弗林。利用基于单因素实验进行的正交实验研究最佳分离工艺,通过紫外分析、原子力显微镜表征证实了P204/正辛醇反胶束体系萃取分离L-辛弗林的有效性。结果萃取最佳工艺条件为：水相pH值6.5、萃取时间15 min、P204浓度0.10mol/L、W_0=5,此条件下L-辛弗林的单次萃取率为68.02%,各影响因素影响顺序为：水相pH〉P204浓度〉W_0〉萃取时间。纯化后的L-辛弗林纯度达到87.8%,比原料纯度提升了2.9倍。结论该方法为L-辛弗林的分离提取提供一种快速低成本方法,并对其萃取机制及主要变化规律方面提供了基础数据。 |
| Author | 桑鲁燕 陶仁友 周小华 王亚文 |
| AuthorAffiliation | 菏泽出入境检验检疫局,菏泽274000 重庆大学化学化工学院,重庆400044 |
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| Author_FL | SANG Lu-Yan ZHOU Xiao-Hua WANG Ya-Wen TAO Ren-You |
| Author_FL_xml | – sequence: 1 fullname: SANG Lu-Yan – sequence: 2 fullname: TAO Ren-You – sequence: 3 fullname: ZHOU Xiao-Hua – sequence: 4 fullname: WANG Ya-Wen |
| Author_xml | – sequence: 1 fullname: 桑鲁燕 陶仁友 周小华 王亚文 |
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| Copyright | Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
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| DocumentTitleAlternate | Extraction of L-synephrine by P204/octanol reverse micelles |
| DocumentTitle_FL | Extraction of L-synephrine by P204/octanol reverse micelles |
| EndPage | 1431 |
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| Keywords | L-辛弗林 萃取 反胶束 reverse micellar extraction L-synephrine |
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| Notes | L-synephrine; reverse micellar; extraction Objective To establish a method of reverse micelle extraction for L-synephrine, and prove the efficiency of extraction by P204/octanol reverse micelle. Methods P204/octanol was chosen and prepared for extracting L-synephrine, which was extracted from fructus. Purified L-synephrine was prepared after reverse extraction, concentration and drying. The optimal conditions of extraction were studied by orthogonal experiment based on single factor experiment. The efficiency of extraction by P204/octanol reverse micelle was proved by UV and AFM spectrum. Results The optimum conditions of extraction were as follows： p H of 6.5, extraction time of 15 min, P204 concentration of 0.10 mol/L, and W_0 of 5. The extraction rate was 68.02% at the optimum conditions for one time, and the effecting order was pHP〉204 concentration〉W0〉extraction time. The purified L-synephrine in reverse extraction was 87.8% after concentration and drying, which was 2.9 times as the raw material. Conclusi |
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| PublicationTitle | 食品安全质量检测学报 |
| PublicationTitleAlternate | Journal of Food Safety and Quality |
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| PublicationYear | 2016 |
| Publisher | 菏泽出入境检验检疫局,菏泽,274000%重庆大学化学化工学院,重庆,400044 |
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| SubjectTerms | L-辛弗林 反胶束 萃取 |
| Title | P204/正辛醇反胶束萃取L-辛弗林的研究 |
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